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Nuclear Forensic Analysis, Second Edition, 2nd Edition
book

Nuclear Forensic Analysis, Second Edition, 2nd Edition

by Kenton J. Moody, Patrick M. Grant, Ian D. Hutcheon
December 2014
Intermediate to advanced content levelIntermediate to advanced
524 pages
20h 21m
English
CRC Press
Content preview from Nuclear Forensic Analysis, Second Edition, 2nd Edition
355Laboratory Analyses
For conventional SEM analysis, samples must be nonvolatile in order to survive
t
he
h
igh-vacuum
e
nvironment
a
nd
c
onductive
t
o
p
revent
c
harging
b
y
t
he
i
ncident
e
lectron
b
eam.
N
onconductive
s
amples
a
re
t
ypically
c
oated
w
ith
a
t
hin
(
2–10nm)
l
ayer
o
f
C
,
A
u,
o
r
I
r.
T
hese
r
equirements
a
re
e
ased
w
ith
a
n
E
SEM,
w
hich
ca
n
o
per-
ate
u
nder
v
arious
s
ample-chamber
at
mospheres.
P
owdered
s
amples
a
re
t
ypically
adhered to a specimen stub using conductive tape or adhesive, or set into epoxy
r
esin
a
nd
p
olished.
A
nalysts
m
ust
t
ake
p
articular
ca
re
t
o
e
nsure
t
hat
t
he
s
ample
i
s
a
dequately
d
ispersed.
C
ommon
me
thods
o
f
d
ispersion
i
nclude
s
onication
us
ing
v
ari-
ous
s
olvents
a
nd
r
epeated
c
ontact
t
ransfers.
D
ispersion
w
ill
d
epend
he
avily ...
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Publisher Resources

ISBN: 9781439880616