book

Pharmaceutical Analysis

by P. D. Chaithanya Sudha

July 2012

Intermediate to advanced

758 pages

17h 12m

English

Pearson India

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IntroductionIntroduction to TitrimetryIntroduction to Electroanalytical MethodsIntroduction to SpectroscopyIntroduction to ChromatographyStatistical AnalysisReview Questions

IntroductionClassification of SolutionsFactors Affecting SolubilityTheoryApplicationsReview Questions
IntroductionReview Questions
IntroductionFactors Affecting ViscosityTypes of ViscometersUnits for the ViscosityApplicationsReview Questions
IntroductionFactors Affecting Surface TensionMethods for Determining Surface TensionApplicationsReview Questions
IntroductionMethods for Particle Size AnalysisApplicationsReview Questions
IntroductionPrincipleTheoryInstrumentationTypes of X-ray Diffraction MethodsAdvantagesDisadvantagesApplicationsReview Questions
IntroductionTheoryConcept of the Circular Dichroism (CD) and Optical Rotatory Dispersion (ORD)InstrumentationApplicationsAdvantagesDisadvantagesReview Questions
IntroductionPrinciple and TheoryInstrumentationFactors Affecting the Refractive IndexApplicationsReview Questions
IntroductionAcid-base ConceptRole of the SolventStrengths of Acids and BasesLaw of Mass ActionHanderson-Hesselbach EquationTypes of Acid-base Titrations and Titration CurvesIndicatorsApplicationsReview Questions
IntroductionPrincipleTheoryTypes of Non-aqueous SolventsPreperation and Standardisation of Standard SolutionsFactors Affecting the Non-aqueous TitrationsDifferent Theories of Non-aqueous TitrationsInterference of the Water in Non-aqueous TitrimetryAdvantagesDisadvantagesApplicationsReview Questions
IntroductionPrincipleTheoryOxidising and Reducing AgentsFactors Affecting Redox TitrationsRedox IndicatorsTypes of Redox TitrationsTitration CurveProcedure Followed for Redox TitrationApplicationsReview Questions
IntroductionPrincipleTheoryProcedureEnd Point DetectionFactors Affecting the DiazotizationConditions for the Diazotization TitrationAdvantagesDisadvantagesApplicationsReview Questions
IntroductionPrincipleTheoryLigandsChelating AgentsDetermination of the End PointEnd Point Detection MethodsTypes of Complexometric TitrationsConcept of Werner Co-ordination NumberConcept of Masking and Demasking AgentsFactors Affecting the Titration ValuesApplicationsReview Questions
IntroductionPrincipleTheoryMechanism of the PrecipitationTypes of GravimetryImpurities Present in the PrecipitatesAdvantagesDisadvantagesApplicationsReview Questions
IntroductionTheoryTypes of the Precipitation TitrationsFactors Affecting the Precipitation TitrationsAdvantagesDisadvantagesApplicationsReview Questions
ArgentometryAdvantagesDisadvantagesApplicationsIodometry and IodimetryApplicationsReview Questions
IntroductionPrincipleTheoryApplicationsReview Questions
IntroductionPrincipleTheoryApparatusMethodFactors Affecting the Conductivity MeasurementsAdvantagesDisadvantagesApplicationsReview Questions
IntroductionPrincipleTheoryInstrumentationApplicationsReview Questions
IntroductionPrincipleTheoryElectrodesPotentiometric TitrationsInstrumentsAdvantagesDisadvantagesApplicationsReview Questions
IntroductionPolarographyAdvantagesDisadvantagesApplicationsAmperometryAdvantagesDisadvantagesApplicationsReview Questions
IntroductionThe Electromagnetic SpectrumTheoryBeer–Lamber's LawInstrumentationSpectrophotometersThe Origins of Absorption SpectraSolvent EffectsSelection of SolventsGood Operating PracticeSources of ErrorApplicationsExperimentsReview Questions
IntroductionTheoryTypes of VibrationsInstrumentationInterpretation of the IR SpectraLimitations of IR SpectroscopyAdvantagesDisadvantagesApplications of IR SpectroscopyFourier Transform Infrared Spectroscopy (FTIR)IntroductionPrincipleInstrumentationAdvantages of FTIRLimitations of FTIRApplicationsReview Questions
IntroductionPrincipleTheoryTypes of FluorescenceInstrumentationFactors Affecting the Fluorescence IntensityConcept of QuenchingFluorescence SpectrumAdvantagesLimitationsApplicationsReview QuestionsX-ray Fluorescence SpectroscopyIntroductionTheoryInstrumentationAdvantagesDisadvantagesApplicationsReview Questions
IntroductionPrincipleTheoryInstrumentationInterferences in AASAdvantagesDisadvantagesApplicationsReview Questions
IntroductionPrinciple and TheoryPrincipleInstrumentation for Flame PhotometryApplications of Flame PhotometryInterferences in Quantitative DeterminationsMerits and Limitations of Flame PhotometryLimitationsAdvantagesReview Questions
IntroductionPrincipleTheoryInstrumentationAdvantagesDisadvantagesAdvantagesDisadvantagesAdvantagesDisadvantagesTypes of Mass SpectrometryAdvantagesDisadvantagesApplicationsReview Questions
IntroductionPrinciple and TheoryChemical ShiftInstrumentationSolvents RequirementsAdvantagesDisadvantagesApplicationsReview Questions
IntroductionTheoryRelaxation and SaturationInstrumentationDouble Resonance SpectrometersInterpretation of Derivative Curves in ESRApplicationsAdvantagesDisadvantagesReview Questions
IntroductionPrincipleTheoryInstrumentationAdvantagesLimitationsApplicationsReview Questions
IntroductionPrincipleTheoryFactors Affecting MeasurementInstrumentationApplications of Nephlometry and TurbidimetryReview Questions
IntroductionPrincipleTheoryTypes of Paper ChromatographyDetection of the Spots in Paper ChromatographyAdvantagesDisadvantagesApplicationsReview Questions
IntroductionPrincipleTheoryFactors Affecting the Column EfficiencyAdvantagesDisadvantagesApplicationsReview Questions
IntroductionPrincipleTheoryThe Process of TLCAdvantages of TLC Over Other TechniquesDisadvantages of TLCTrouble Shooting in TLCApplicationsReview Questions
IntroductionTypes of HPLC TechniquesInstrumentation for HPLCThe Rate Theory of ChromatographyAdvantages of HPLCDisadvantages of HPLCHPLC Trouble ShootingApplications of HPLCReview Questions
IntroductionPrincipleTheoryInstrumental Components (or) InstrumentationIon Exchange Resins Efficiency ParametersAdvantages of IECApplicationsReview Questions
IntroductionPrinciple and TheoryTypes of GCInstrumentationFactors that Affect GC SeparationsParametersAdvantagesDisadvantagesApplicationsReview Questions
IntroductionTheoryInstrumentationParameters Checked for the VPCProcedureFactors Effecting Elution Time and Resolution PowerApplicationsReview Questions
IntroductionTheoryImportant Properties of SCFsAdvantagesDisadvantagesInstrumentationCategorisation of SFCAdvantages of SCF Over HPLC and GCLimitationsPrecautionsComparison of SFC with HPLC and GCApplications of SFCReview Questions
IntroductionClassification of Affinity ChromatographyGeneral Procedure for the Development of Affinity ChromatographyAdvantages of Affinity ChromatographyFactors Affecting Affinity Chromatographic SeparationType of MatricesApplicationsReview Questions
IntroductionPrincipleInstrumentationSample InjectionDetectorsComparison Between Well Established On-line Two-dimensional Nano LC-MS and Off-line Two-dimensional NANO LC-MSAdvantagesApplicationsReview Questions
IntroductionPrincipleTheoryTypes of ElectrophoresisInstrumentationElution MethodFactors Affecting the ElectrophoresisAdvantagesDisadvantagesApplicationsReview Questions
IntroductionPrincipleTheoryInstrumentationElution ProcedureColumn ParametersFactors Affecting SEC SeparationsAdvantages of SECDisadvantages of SECApplicationsGel Permeation ChromatographyFactors Affecting GPC SeparationAdvantages of GPCDisadvantagesApplicationsReview Questions
IntroductionStructureMechanism of ActionOxidising Agent Used for Colour Production with MBTHFactors Affecting Nature and Intensity of ColourAdvantages of MBTHReview Questions
IntroductionStructureMechanism of ActionPreparationApplicationsReview Questions
IntroductionStructuresMechanism of ActionApplicationsReview Questions
IntroductionStructureProcedure for DeterminationsMechanism of ActionReview Questions
IntroductionStructureMechanism of ActionProcedurePreparation of NQSApplicationsMechanism of ActionProcedureReview Questions
IntroductionStructureMechanism of ActionPreparation of BM ReagentReview Questions
IntroductionStructureMechanism of ActionPreparationStorageApplicationsReview Questions
IntroductionStructureMechanism of ActionApplicationsReview Questions
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IntroductionReview Questions
IntroductionReview Questions
IntroductionReview Questions
IntroductionReview Questions
IntroductionReview Questions
IntroductionReview Questions
IntroductionClassificationReview Questions
DefinitionReview Questions
IntroductionAnalysis MethodsReview Questions
IntroductionReview Questions
Review Questions
IntroductionAnalytical Methods for DiureticsReview Questions
IntroductionReview Questions
Review Questions
IntroductionClassificationAnalysis of VitaminAnalysis Vitamin B1 (Thiamine)Analysis of Vitamin B2 (Riboflavin)Analysis of Vitamin B6 (Pyridoxine Hydrochloride)Analysis of Vitamin B12 (Cyanocobalamin)Analysis of Pantothenic AcidAnalysis of Nicotinic Acid and NicotinamideAnalysis of Vitamin C (Ascorbic Acid)Analysis of Vitamin D (Calciferol)Analysis of Vitamin KAnalysis of p-Amino Benzoic Acid (Vitamin B4)Analysis of Folic AcidAnalysis of Vitamin EReview Questions
IntroductionReview Questions
Chemical TestsReview Questions
IntroductionReview Questions
IntroductionAdvantagesLimitationsApplicationsAdvantageLimitationAdvantagesDisadvantagesApplicationsReview Questions
IntroductionGeneral Procedure for the ElisaAdvantagesApplicationsBioassaysReview Questions
IntroductionThermogravimetryDifferential Thermal AnalysisDifferential Scanning CalorimetryReview Questions
IntroductionMoisture Content DeterminationProcedureReview Questions
Crude Protein Analysis (Nitrogen Determination)CarbohydratesAnalysis of Lipids (Oils and Fats)Review Questions
IntroductionReview Questions
Quality Assurance (QA)New Drug ApplicationAbbreviated New Drug ApplicationDefinition of INDDocumentation
IntroductionTypes of ValidationValidation of Air Handling SystemsValidation of Water Handling System

Content preview from Pharmaceutical Analysis

Multiple-choice Questions

II. PHYSICAL ANALYTICAL METHODS

Solubility Determinations
1. Which one of the following is most soluble in the water?
  1. CH₃CH₂OH
  2. CH₃CH₂CH₂OH
  3. CH₃OH
  4. CH₃CH₂CH₂CH₂OH
2. Which of the following statement is true?
  1. Solubility of gases are increased with the temperature increase
  2. Solubility of the solids are decreased with the temperature increase
  3. Solubility of the gases are increased with the temperature increase
  4. Solubility of the solids are increased with the temperature increase
3. Silver carbonate is most soluble in_________.
  1. sodium carbonate
  2. nitric acid
  3. silver nitrate
  4. silver chloride
4. Calculate the molality by dissolving the 12 g of the benzene in the 38 g of carbon tetra chloride_______.
  1. 0.316 m
  2. 0.508 m
  3. 0.622 m
  4. 0.240 m
5. The solubility ...