book

Analysis, Synthesis, and Design of Chemical Processes, Fourth Edition

Name: Analysis, Synthesis, and Design of Chemical Processes, Fourth Edition
ISBN: 9780132618724

by Richard Turton, Richard C. Bailie, Wallace B. Whiting, Joseph A. Shaeiwitz, Debangsu Bhattacharyya

June 2012

Intermediate to advanced

1104 pages

38h 56m

English

Pearson

Read now

Unlock full access

Title Page
Copyright Page
Contents
Material on the CD-ROM
Preface
About the Authors
List of Nomenclature
Section I. Conceptualization and Analysis of Chemical Processes
Chapter 1. Diagrams for Understanding Chemical Processes
1.1. Block Flow Diagram (BFD)1.2. Process Flow Diagram (PFD)1.3. Piping and Instrumentation Diagram (P&ID)1.4. Additional Diagrams1.5. Three-Dimensional Representation of a Process1.6. The 3-D Plant Model1.7. Operator and 3-D Immersive Training Simulators1.8. SummaryReferencesShort Answer QuestionsProblems
Chapter 2. The Structure and Synthesis of Process Flow Diagrams
2.1. Hierarchy of Process Design2.2. Step 1—Batch Versus Continuous Process2.3. Step 2—The Input/Output Structure of the Process2.4. Step 3—The Recycle Structure of the Process2.5. Step 4—General Structure of the Separation System2.6. Step 5—Heat-Exchanger Network or Process Energy Recovery System2.7. Information Required and Sources2.8. SummaryReferencesShort Answer QuestionsProblems

Chapter 3. Batch Processing
3.1. Design Calculations for Batch Processes3.2. Gantt Charts and Scheduling3.3. Nonoverlapping Operations, Overlapping Operations, and Cycle Times3.4. Flowshop and Jobshop Plants3.5. Product and Intermediate Storage and Parallel Process Units3.6. Design of Equipment for Multiproduct Batch Processes3.7. SummaryReferencesShort Answer QuestionsProblems
Chapter 4. Chemical Product Design
4.1. Strategies for Chemical Product Design4.2. Needs4.3. Ideas4.4. Selection4.5. Manufacture4.6. Batch Processing4.7. Economic Considerations4.8. SummaryReferences
Chapter 5. Tracing Chemicals through the Process Flow Diagram
5.1. Guidelines and Tactics for Tracing Chemicals5.2. Tracing Primary Paths Taken by Chemicals in a Chemical Process5.3. Recycle and Bypass Streams5.4. Tracing Nonreacting Chemicals5.5. Limitations5.6. Written Process Description5.7. SummaryProblems
Chapter 6. Understanding Process Conditions
6.1. Conditions of Special Concern for the Operation of Separation and Reactor Systems6.2. Reasons for Operating at Conditions of Special Concern6.3. Conditions of Special Concern for the Operation of Other Equipment6.4. Analysis of Important Process Conditions6.5. SummaryReferencesShort Answer QuestionsProblems
Section II. Engineering Economic Analysis of Chemical Processes
Chapter 7. Estimation of Capital Costs
7.1. Classifications of Capital Cost Estimates7.2. Estimation of Purchased Equipment Costs7.3. Estimating the Total Capital Cost of a Plant7.4. SummaryReferencesShort Answer QuestionsProblems
Chapter 8. Estimation of Manufacturing Costs
8.1. Factors Affecting the Cost of Manufacturing a Chemical Product8.2. Cost of Operating Labor8.3. Utility Costs8.4. Raw Material Costs8.5. Yearly Costs and Stream Factors8.6. Estimating Utility Costs from the PFD8.7. Cost of Treating Liquid and Solid Waste Streams8.8. Evaluation of Cost of Manufacture for the Production of Benzene Via the Hydrodealkylation of Toluene8.9. SummaryReferencesShort Answer QuestionsProblems
Chapter 9. Engineering Economic Analysis
9.1. Investments and the Time Value of Money9.2. Different Types of Interest9.3. Time Basis for Compound Interest Calculations9.4. Cash Flow Diagrams9.5. Calculations from Cash Flow Diagrams9.6. Inflation9.7. Depreciation of Capital Investment9.8. Taxation, Cash Flow, and Profit9.9. SummaryReferencesShort Answer QuestionsProblems
Chapter 10. Profitability Analysis
10.1. A Typical Cash Flow Diagram for a New Project10.2. Profitability Criteria for Project Evaluation10.3. Comparing Several Large Projects: Incremental Economic Analysis10.4. Establishing Acceptable Returns from Investments: The Concept of Risk10.5. Evaluation of Equipment Alternatives10.6. Incremental Analysis for Retrofitting Facilities10.7. Evaluation of Risk in Evaluating Profitability10.8. Profit Margin Analysis10.9. SummaryReferencesShort Answer QuestionsProblems
Section III. Synthesis and Optimization of Chemical Processes
Chapter 11. Utilizing Experience-Based Principles to Confirm the Suitability of a Process Design
11.1. The Role of Experience in the Design Process11.2. Presentation of Tables of Technical Heuristics and Guidelines11.3. SummaryReferencesProblems
Chapter 12. Synthesis of the PFD from the Generic BFD
12.1. Information Needs and Sources12.2. Reactor Section12.3. Separator Section12.4. Reactor Feed Preparation and Separator Feed Preparation Sections12.5. Recycle Section12.6. Environmental Control Section12.7. Major Process Control Loops12.8. Flow Summary Table12.9. Major Equipment Summary Table12.10. SummaryReferencesGeneral ReferenceProblems
Chapter 13. Synthesis of a Process Using a Simulator and Simulator Troubleshooting
13.1. The Structure of a Process Simulator13.2. Information Required to Complete a Process Simulation: Input Data13.3. Handling Recycle Streams13.4. Choosing Thermodynamic Models13.5. Case Study: Toluene Hydrodealkylation Process13.6. Electrolyte Systems Modeling13.7. Solids ModelingAppendix 13.1. Calculation of Excess Gibbs Energy for Electrolyte SystemsAppendix 13.2. Steps to Build a Model of a Distillation Column for an Electrolyte System Using a Rate-Based Simulation with a Film Model for Mass Transfer, the Parameters Required at Each Stage, and Possible Sources of These Parameters13.8. SummaryReferencesShort Answer QuestionsProblems
Chapter 14. Process Optimization
14.1. Background Information on Optimization14.2. Strategies14.3. Topological Optimization14.4. Parametric Optimization14.5. Lattice Search Techniques versus Response Surface Techniques14.6. Process Flexibility and the Sensitivity of the Optimum14.7. Optimization in Batch Systems14.8. SummaryReferencesShort Answer QuestionsProblems
Chapter 15. Pinch Technology
15.1. Introduction15.2. Heat Integration and Network Design15.3. Composite Temperature-Enthalpy Diagram15.4. Composite Enthalpy Curves for Systems without a Pinch15.5. Using the Composite Enthalpy Curve to Estimate Heat-Exchanger Surface Area15.6. Effectiveness Factor (F) and the Number of Shells15.7. Combining Costs to Give the Eaoc for the Network15.8. Other Considerations15.9. Heat-Exchanger Network Synthesis Analysis and Design (HENSAD) Program15.10. Mass-Exchange Networks15.11. SummaryReferencesShort Answer QuestionsProblems
Chapter 16. Advanced Topics Using Steady-State Simulators
16.1. Why the Need for Advanced Topics in Steady-State Simulation?16.2. User-Added Models16.3. Solution Strategy for Steady-State Simulations16.4. Studies with the Steady-State Simulation16.5. Estimation of Physical Property Parameters16.6. SummaryReferencesShort Answer QuestionsProblems
Chapter 17. Using Dynamic Simulators in Process Design
17.1. Why is there a Need for Dynamic Simulation?17.2. Setting Up a Dynamic Simulation17.3. Dynamic Simulation Solution Methods17.4. Process Control17.5. SummaryReferencesShort Answer QuestionsProblems
Chapter 18. Regulation and Control of Chemical Processes with Applications Using Commercial Software
18.1. A Simple Regulation Problem18.2. The Characteristics of Regulating Valves18.3. Regulating Flowrates and Pressures18.4. The Measurement of Process Variables18.5. Common Control Strategies Used in Chemical Processes18.6. Exchanging Heat and Work Between Process and Utility Streams18.7. Logic Control18.8. Advanced Process Control18.9. Case Studies18.10. Putting it all Together: The Operator Training Simulator (OTS)18.11. SummaryReferencesProblems
Section IV. Analysis of Process Performance
Chapter 19. Process Input/Output Models
19.1. Representation of Process Inputs and Outputs19.2. Analysis of the Effect of Process Inputs on Process Outputs19.3. A Process Example19.4. SummaryProblems
Chapter 20. Tools for Evaluating Process Performance
20.1. Key Relationships20.2. Thinking with Equations20.3. Base-Case Ratios20.4. Analysis of Systems Using Controlling Resistances20.5. Graphical Representations20.6. SummaryReferenceProblems
Chapter 21. Performance Curves for Individual Unit Operations
21.1. Application to Heat Transfer21.2. Application to Fluid Flow21.3. Application to Separation Problems21.4. SummaryReferenceShort Answer QuestionsProblems
Chapter 22. Performance of Multiple Unit Operations
22.1. Analysis of a Reactor with Heat Transfer22.2. Performance of a Distillation Column22.3. Performance of a Heating Loop22.4. Performance of the Feed Section to a Process22.5. SummaryReferencesShort Answer QuestionsProblems
Chapter 23. Reactor Performance
23.1. Production of Desired Product23.2. Reaction Kinetics and Thermodynamics23.3. The Chemical Reactor23.4. Heat Transfer in the Chemical Reactor23.5. Reactor System Case Studies23.6. SummaryReferencesShort Answer QuestionsProblems
Chapter 24. Process Troubleshooting and Debottlenecking
24.1. Recommended Methodology24.2. Troubleshooting Individual Units24.3. Troubleshooting Multiple Units24.4. A Process Troubleshooting Problem24.5. Debottlenecking Problems24.6. SummaryReferencesProblems
Section V. The Impact of Chemical Engineering Design on Society
Chapter 25. Ethics and Professionalism
25.1. Ethics25.2. Professional Registration25.3. Legal Liability [13]25.4. Business Codes of Conduct [14, 15]25.5. SummaryReferencesProblems
Chapter 26. Health, Safety, and the Environment
26.1. Risk Assessment26.2. Regulations and Agencies26.3. Fires and Explosions26.4. Process Hazard Analysis26.5. Chemical Safety and Hazard Investigation Board26.6. Inherently Safe Design26.7. Summary26.8. GlossaryReferencesProblems
Chapter 27. Green Engineering
27.1. Environmental Regulations27.2. Environmental Fate of Chemicals27.3. Green Chemistry27.4. Pollution Prevention During Process Design27.5. Analysis of a PFD for Pollution Performance and Environmental Performance27.6. An Example of the Economics of Pollution Prevention27.7. Life Cycle Analysis27.8. SummaryReferencesProblems
Section VI. Interpersonal and Communication Skills
Chapter 28. Teamwork
28.1. Groups28.2. Group Evolution28.3. Teams and Teamwork28.4. Misconceptions28.5. Learning in Teams28.6. Other Reading28.7. SummaryReferencesProblems
Appendix A. Cost Equations and Curves for the CAPCOST Program
A.1. Purchased Equipment CostsA.2. Pressure FactorsA.3. Material Factors And Bare Module FactorsReferences
Index
Chapter 0. Outcomes Assessment
0.1. Student Self-Assessment0.2. Assessment by Faculty0.3. SummaryReferencesOther References
Chapter 29. Written and Oral Communication
29.1. Audience Analysis29.2. Written Communication29.3. Oral Communication29.4. Software and Author Responsibility29.5. SummaryReferencesProblems
Chapter 30. A Report-Writing Case Study
30.1. The Assignment Memorandum30.2. Response Memorandum30.3. Visual Aids30.4. Example Reports30.5. Checklist of Common Mistakes and Errors
Appendix B. Information for the Preliminary Design of Fifteen Chemical Processes
B.1. Dimethyl Ether (DME) Production, Unit 200B.2. Ethylbenzene Production, Unit 300B.3. Styrene Production, Unit 400B.4. Drying Oil Production, Unit 500B.5. Production Of Maleic Anhydride From Benzene, Unit 600B.6. Ethylene Oxide Production, Unit 700B.7. Formalin Production, Unit 800B.8. Batch Production Of L-Phenylalanine And L-Aspartic Acid, Unit 900B.9. Acrylic Acid Production Via The Catalytic Partial Oxidation Of Propylene [1, 2, 3, 4, 5], Unit 1000B.10. Production Of Acetone Via The Dehydrogenation Of Isopropyl Alcohol (IPA) [1, 2, 3, 4], Unit 1100B.11. Production Of Heptenes From Propylene And Butenes [1], Unit 1200B.12. Design of a Shift Reactor Unit to Convert Co To Co2, Unit 1300B.13. Design of a Dual-Stage Selexol Unit to Remove CO2 And H2S From Coal-Derived Synthesis Gas, Unit 1400B.14. Design of a Claus Unit For the Conversion of H2s to Elemental Sulfur, Unit 1500B.15. Modeling a Downward-Flow, Oxygen-Blown, Entrained-Flow Gasifier, Unit 1600
Appendix C. Design Projects
Project 1. Increasing the Production of 3-Chloro-1-Propene (Allyl Chloride) in Unit 600PROJECT 2. Design and Optimization of a New 20,000-Metric-Tons-per-Year Facility to Produce Allyl Chloride at La Nueva Cantina, MexicoPROJECT 3. Scale-Down of Phthalic Anhydride Production at TBWS Unit 700PROJECT 4. The Design of a New 100,000-Metric-Tons-per-Year Phthalic Anhydride Production FacilityPROJECT 5. Problems at the Cumene Production Facility, Unit 800PROJECT 6. Design of a New, 100,000-Metric-Tons-per-Year Cumene Production Facility
Where are the Companion Content Files?

Content preview from Analysis, Synthesis, and Design of Chemical Processes, Fourth Edition

Material on the CD-ROM

Preface

About the Authors

List of Nomenclature

SECTION I CONCEPTUALIZATION AND ANALYSIS OF CHEMICAL PROCESSES

Chapter 1 Diagrams for Understanding Chemical Processes

What You Will Learn

1.1 Block Flow Diagram (BFD)

1.1.1 Block Flow Process Diagram

1.1.2 Block Flow Plant Diagram

1.2 Process Flow Diagram (PFD)

1.2.1 Process Topology

1.2.2 Stream Information

1.2.3 Equipment Information

1.2.4 Combining Topology, Stream Data, and Control Strategy to Give a PFD

1.3 Piping and Instrumentation Diagram (P&ID)

1.4 Additional Diagrams

1.5 Three-Dimensional Representation of a Process

1.6 The 3-D Plant Model

1.7 Operator and 3-D Immersive Training Simulators

1.7.1 Operator Training Simulators (OTS)

1.7.2 3-D Immersive Training ...

Become an O’Reilly member and get unlimited access to this title plus top books and audiobooks from O’Reilly and nearly 200 top publishers, thousands of courses curated by job role, 150+ live events each month,
and much more.

Read now

Unlock full access

More than 5,000 organizations count on O’Reilly

O’Reilly covers everything we've got, with content to help us build a world-class technology community, upgrade the capabilities and competencies of our teams, and improve overall team performance as well as their engagement.

Julian F.

Head of Cybersecurity

I wanted to learn C and C++, but it didn't click for me until I picked up an O'Reilly book. When I went on the O’Reilly platform, I was astonished to find all the books there, plus live events and sandboxes so you could play around with the technology.

Addison B.

Field Engineer

I’ve been on the O’Reilly platform for more than eight years. I use a couple of learning platforms, but I'm on O'Reilly more than anybody else. When you're there, you start learning. I'm never disappointed.

Amir M.

Data Platform Tech Lead

I'm always learning. So when I got on to O'Reilly, I was like a kid in a candy store. There are playlists. There are answers. There's on-demand training. It's worth its weight in gold, in terms of what it allows me to do.

Mark W.

Embedded Software Engineer

Elements of Chemical Reaction Engineering, 7th Edition

Publisher Resources

ISBN: 9780132618724Purchase book

Cloud Computing

Data Engineering

Data Science

AI & ML

Programming Languages

Software Architecture

IT/Ops

Security

Design

Business

Soft Skills

Analysis, Synthesis, and Design of Chemical Processes, Fourth Edition

by Richard Turton, Richard C. Bailie, Wallace B. Whiting, Joseph A. Shaeiwitz, Debangsu Bhattacharyya

Contents

Become an O’Reilly member and get unlimited access to this title plus top books and audiobooks from O’Reilly and nearly 200 top publishers, thousands of courses curated by job role, 150+ live events each month,
and much more.