
61Nanostructured MetalOxides andGas-Sensing Devices
500 nm
(a)
(b)
[111]
–
[111]
20 nm
(c)
2.52 Å
2.32 Å
FIGURE 7.13
(a) SEM and (b) TEM images of CuO nanowires synthesized by heating copper wire, of 0.1 mm
diameter, in air to a temperature of 500°C for 4 h. Each CuO nanowire was a bicrystal as shown
by its electron diffraction pattern and HRTEM characterization. (c) HRTEM image showing
the twin boundary of a nanowire. (From Xia, Y., Yang, P., Sun, Y., Wu, Y., Mayers, B., Gates, B.,
Yin, Y., Kim, F., and Yan, H.: One-dimensional nanostructures: Synthesis, characterization, and
applications. Adv. Mater. 2003. 15. 353–389. Copyright Wiley-VCH Verlag GmbH ...