
232.5 Results and discussion
ratio CO
2
:CO 23,000 (
O
2
1 10
16
atm). The actual mixing ratios used in this
work turned out to be 0.2% CO
2
99.8% CO in the rst case and 43 ppm CO
balance CO
2
in the second case. In order to generate the later mixture, a gas cylinder
containing 100 ppm CO balance CO
2
was used as the CO source. A similar strat-
egy was adopted in the case of oxygen partial pressure modulation in WO
3
in the
light of the theoretical data illustrated in Figure 2.1c.
In the case of titania thick lms electrodeposited on cp Ti plates and wires, the
calcined samples were subjected to reduction experiment in 5% H
2
/Ar mixture ...